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:: Volume 25, Number 2 (7-2017) ::
2017, 25(2): 427-438 Back to browse issues page
The effect of PbO nanoparticles on structural and microstructure of Bi2-xPbxSr2Ca2Cu4Oy superconductor composition
Abstract:   (59 Views)

In this paper, β-PbO nanoparticles were prepared by microwave irradiation. Then, the PbO nanoparticles with size of 32 nm were doped in the Bi2-xPbxSr2Ca2Cu4Oy superconductor with x = 0.0, 0.2, 0.4 and 0.6. The samples were synthesized by the standard solid state reaction method. The structural properties, microstructure and morphology of the samples have been studied by XRD and SEM. After synthesizing the samples and observing the Meissner effect, the study of the critical current density (Jc), critical temperature (Tc) and thermogravimetry-differential thermal analysis shows that samples have been down. The results of the critical current density measurements show that the sample with x = 0.4 and an annealing time 60 h has the maximum Jc. Substitution of PbO nanoparticles for Bi reveal that remarkable increases in the critical temperature. The volume of the unit cell of doped samples were increased with respect to that of the undoped samples, which is shown Bi+3 substituted by Pb+2.

Keywords: Nanoparticles of PbO, superconductivity, critical current density, structural and microstructure.
Full-Text [PDF 131 kb]   (33 Downloads)    
Type of Study: Research | Subject: Special
Received: 2017/06/13 | Accepted: 2017/06/13 | Published: 2017/06/13
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The effect of PbO nanoparticles on structural and microstructure of Bi2-xPbxSr2Ca2Cu4Oy superconductor composition . Iranian Journal of Crystallography and Mineralogy. 2017; 25 (2) :427-438
URL: http://ijcm.ir/article-1-800-en.html
Volume 25, Number 2 (7-2017) Back to browse issues page
مجله بلورشناسی و کانی شناسی ایران Iranian Journal of Crystallography and Mineralogy
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