Volume 26, Issue 1 (4-2018)                   www.ijcm.ir 2018, 26(1): 251-260 | Back to browse issues page


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Ranjbar, Ghazi, Izadifard. Effect of drying temperature on structural, dielectric, optical and magnetic properties of sol-gel derived BiFeO3 nanoparticles. www.ijcm.ir. 2018; 26 (1) :251-260
URL: http://ijcm.ir/article-1-1065-en.html
Abstract:   (787 Views)
The reaction of 2-hydroxy-3-methoxybenzaldehyde with 4-nitrosulfonylhydrazide under refluxing led to co-crystalline compound contains N'-(2-hydroxy-3-methoxy benzylidene)-4-nitro benzenesulfonylhydrazide (a sulfonamide-Schiff base compound) and 1,2-bis (2-hydroxy-3-methoxy-benzylidenehydrazine) (I). A medium strong hydrogen bonds in 1 links the oxygen atoms of one molecule of 1,2-bis(2-hydroxy-3-methoxy-benzylidenehydrazine) to the NH group of the N'-(2-hydroxy-3-methoxy benzylidene)-4-nitrobenzenesulfonylhydrazide and is responsible for establishing of co-crystals. Compound 1 was characterized by NMR and IR spectroscopy, elemental analysis and single crystal X-ray diffraction method. Crystallographic data for 1 was collected at 95 K.  The synthesized compound has been crystallized in monoclinic system with P21/n space group and a = 6.6771(2) Å, b = 19.2072(6) Å, c = 17.3980(1) Å, β = 95.56(3)º cell parameters. The final R value is 0.037 for 07 independent reflections.
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Type of Study: Research | Subject: Special
Received: 2018/02/28 | Accepted: 2018/02/28 | Published: 2018/02/28

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