Volume 15, Issue 2 (10-2007)
www.ijcm.ir 2007, 15(2): 345-356 |
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Synthesis and characterization ofVO (salen) complex in
Zeolite X Pores. www.ijcm.ir 2007; 15 (2) :345-356
URL: http://ijcm.ir/article-1-817-en.html
URL: http://ijcm.ir/article-1-817-en.html
Abstract: (2744 Views)
In this research, ZeoliteX (Na&6 [(AI02)&6(Si02)u>6].264H20), has
been prepared from 2onouz Kaolin. Then VOX·Zeolite has been obtained by
treatment of ZeoliteX with vanadyl sulfate solution .The Salen ligand has
synthesized by condensation reaction of salisylaldehyde and ethylendiamine.
The encapsulated complex, VO (salen), in zeolite pores was prepared by
reaction of salen with VOX·Zeolite in ethanol at reflux temperatur.The
product was characterized by FT·IR, XRD and SEM (EDX) techniques.
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