Volume 13, Issue 1 (4-2005)
www.ijcm.ir 2005, 13(1): 185-194 |
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Synthesis and Crystal Structure of a Novel Six-Coordinate Gallium (III) Complex. www.ijcm.ir 2005; 13 (1) :185-194
URL: http://ijcm.ir/article-1-735-en.html
URL: http://ijcm.ir/article-1-735-en.html
Abstract: (2891 Views)
The reaction of gallium (III) nitrate octahydrate with the proton transfer compound (pydaH2)2+ (pydc)2– ( where pyda is 2,6-pyridinediamine and pydcH2 is 2,6-pyridinedicarboxylic acid) leads to the formation of (C5H8N3) [Ga(C7H3NO4)2] · 4H2O · CH3OH. The crystal system of the anionic complex is triclinic with space group Pī and two molecules per unit cell. The unit cell parameters are a=10.238(2) Å, b=10.428(2) Å, c=13.838(2) Å, α=70.375(3)°, β=77.938(3)°, γ=64.120(3)°. The structure has been refined to a final value for the crystallographic R factor of 0.0579 based on 4703 reflections with I > 2σ(I).
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