In this paper, Bi1.66Pb0.34Sr2Ca2Cu3O superconductor powders have been prepared via sol-gel and solid-state reaction methods. The structural and magnetic properties have been studied by the X-Ray diffraction (Fullprof analysis) and magnetic susceptibility measurements. The superconductivity and structural properties of the samples have been compared with the properties of a commercially available sample from Aldrich Company.
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