Volume 2, Issue 2 (10-1994)
www.ijcm.ir 1994, 2(2): 1-9 |
Back to browse issues page
Abstract: (3119 Views)
Inc Sm(1)(TIIFh reacts with mcthylllthlUm In TIIF In the
prese nce of lclram c lhyt c lhy lcn c d lamln e, TMEDA , 10 gIve
1[1 .J(l ·MI :I)A)h[Sm«('I I)61}. J'IIF. Tl1c complex has been ch;lractcnzcd
hy elemenl al analyses, lit spectrum and magnetic mcasurem ent .
Molecular .lOd clymsl .SruClUrc of thl! complcx hoo been determmed by a
sIngle cryst .. ! X - ray diffractIOn . The crystalS arc trigonal WIth a =
16.6X4( IO)A , c = 24.946( IO)A , sp<lec group R3c, and SIX molecuies/ulll!
cell. The final It v,.Ilue is 0.043 for 2.140 reneclions measured.
Keywords: Preparllfion, MolecullIr SlrnClllrt', {I Li(TMEDA )/1.ISm(
CJ-I1h.n. TflF, JR SpeClrnm, Magnetic Measllremem
| Rights and permissions | |
 |
This work is licensed under a Creative Commons Attribution-NonCommercial 4.0 International License. |