Volume 22, Issue 1 (4-2014)
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Synthesis, Characterization and Crystal structure of Chiral Schiff base compound (E)-3, 4-Dimethoxy [(1-phenylethyl) iminomethyl] benzyne. www.ijcm.ir 2014; 22 (1) :1-6
URL: http://ijcm.ir/article-1-263-en.html
URL: http://ijcm.ir/article-1-263-en.html
Abstract: (2801 Views)
The crystal structure of the title chiral Schiff base compound (E)-3,4-dimethoxy[(1-phenylethyl)iminomethyl]bezyne (1) was determined by single-crystal X-ray diffraction data. The title compound was further characterized by elemental analyses (CHN), FT-IR, 1H-NMR and UV-Vis spectroscopic techniques. It crystallizes in the monoclinic space group P21 with unit cell parameters:
a = 19.0121 (2), b = 8.2507 (2), c = 9.7331 (4) Ǻ, β = 92.488 (2)°, V = 1525.33 (7) Ǻ3, Z = 4, R1 = 0.0299, wR2 = 0.787, R1 = 0.0329, wR2 = 0.0804.
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