in this research, Complex (o.l(phcnh(N03hl was
synthesizcd and the structure was determined by
single-crystal X-ray diffraction method. This complex was
synthesized by using 1, 10 - Phcnanthrolinc and each of
complexes ]Cd(Meurea)61(NO,h and [Cd(urea),(NO,hl at
50-600C. This complex crystallizes in triclinic crystal system,
space group P( -. )(2) with two molecules in the unit cell.
Laaice parameters of this compound are:
a= 9.6008(5)A h= 9.6044(3)A c= 13.4376(1I)A
a= 99.5624(4)° (J= 99.5564(6)° y= 105.0862(3)"
V= 1152.65(13)A D,",,= 1.7221 mglm'
After structural determination, Rand Rw constants
decreased to 0.0772 and 0.0935 respectively. The Cd atom
in this complex was eight-coordinated. In addition, If and
XRD studies also carried out.
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