دوره 26، شماره 4 - ( 10-1397 )
جلد 26 شماره 4 صفحات 1036-1027 |
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pormehr A, Niyaifar M, Hassanpour A. Investigation of structural properties of Yttrium Iron Garnet substituted by Antimony fabricated via sol-gel method. www.ijcm.ir 2019; 26 (4) :1027-1036
URL: http://ijcm.ir/article-1-1208-fa.html
URL: http://ijcm.ir/article-1-1208-fa.html
پرمهر اسماء، نیایی فر محمد، حسن پور احمد. اثر جانشانی آنتیموان بر ویژگی ساختاری و مغناطیسی گارنت ایتریوم آهن تهیه‌شده به روش سل ژل. مجله بلورشناسی و کانی شناسی ایران. 1397; 26 (4) :1027-1036
اسماء پرمهر1 
، محمد نیایی فر* 1، احمد حسن پور1
، محمد نیایی فر* 1، احمد حسن پور1
1- دانشگاه آزاد اسلامی
چکیده: (3740 مشاهده)
در این پژوهش نانو بلورکهای گارنت ایتریوم آهن جانشانی شده با آنتیموان با فرمول ساختاری SbxY3-xFe5O12 (Sb-YIG) با 2/0، 1/0، 0x = به روش سل ژل تهیه شدند و اثر جانشانی آنتیموان بر ساختار بلوری توسط پراشسنج پرتوایکس (XRD) و بینابسنجی تبدیل فوریه فروسرخ دور (Far FT-IR) بررسی شد. نتایج نشان داد که نمونهها علاوه بر فاز گارنت دارای فازهای جانبی YFeO3 (YIP)، α-Fe2O3و Sb2O4 بودند و با افزایش مقدار جانشانی، فاز گارنت کاهش یافته است. مقدار فاز گارنت و فازهای ناخالصی محاسبه شد و پس از آن درصد فاز آنتیموان جانشانی شده در جایگاه دوازدهوجهی بدست آمد. در پایان، ویژگیهای مغناطیسی نانوذرات با استفاده از مغناطیسسنج نمونهی ارتعاشی(VSM) بررسی شد که مشخص شد مغناطش اشباع Sb-YIG با افزایش جانشانی کاهش یافته است.
واژه‌های کلیدی: سل ژل، گارنت ایتریوم آهن، آنتیموان، بیناب سنجی تبدیل فوریه فروسرخ دور، مغناطیسسنج نمونهی ارتعاشی.
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